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Analytical chemistry laboratory exercises

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Course Unit Code9360-0123/02
Number of ECTS Credits Allocated3 ECTS credits
Type of Course Unit *Compulsory
Level of Course Unit *First Cycle
Year of Study *Second Year
Semester when the Course Unit is deliveredSummer Semester
Mode of DeliveryFace-to-face
Language of InstructionCzech
Prerequisites and Co-Requisites Course succeeds to compulsory courses of previous semester
Name of Lecturer(s)Personal IDName
OTO30RNDr. Hana Otoupalíková
Summary
Students will try basic gravimetric and volumetric analytical methods and chosen electrochemical and spectral methods.
Learning Outcomes of the Course Unit
The goal is to acquaint students with the procedures of chosen analytical methods.
Course Contents
Fundamentals calculations in analytical chemistry
- Evaluation of analytical results
- Gravimetric determination of sulphates
- Volumetric determination
- Potentiometric titration with ion selective electrode
- Measurement of pH and specific conductivity
- Turbidimetric determination of mud
- Determination of As by flow coulometry
- Atomic absorption spectrometry
- Atomic emission spectrometry with inductively coupled plasma
- X-Ray fluorescence spectrometry
Recommended or Required Reading
Required Reading:
Instruction for laboratory practices.
KENKEL, J., Analytical Chemistry for Technicians, Third Edition CRC 2002
Basic analytical chemistry. 1980.
BENÁTSKÁ, L.: Výpočty v analytické chemii. ES VŠB-TU, Ostrava 1999.
KLIKA, Z., PRAUS, P.: Analytická chemie I. ES VŠB-TU, Ostrava 2002.
Návody k jednotlivým laboratorním cvičením.
KENKEL, J., Analytical Chemistry for Technicians, Third Edition CRC 2002.

Recommended Reading:
KEALEY, David a Peter J. HAINES. Analytical chemistry. Oxford: BIOS, 2002
CHRISTIAN, Gary D. Analytical chemistry. 5th ed. New York: Wiley, c1994. ISBN 0-471-30582-0.
SOMMER, L.: Základy analytické chemie I, VUTIUM, Brno, 1998.
SOMMER, L.: Základy analytické chemie II, VUTIUM, Brno, 2000.
KEALEY, David a Peter J. HAINES. Analytical chemistry. Oxford: BIOS, 2002.
Planned learning activities and teaching methods
Experimental work in labs
Assesment methods and criteria
Task TitleTask TypeMaximum Number of Points
(Act. for Subtasks)
Minimum Number of Points for Task Passing
Graded creditGraded credit100 51