| Course Unit Code | 9360-0139/01 |
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| Number of ECTS Credits Allocated | 3 ECTS credits |
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| Type of Course Unit * | Compulsory |
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| Level of Course Unit * | First Cycle |
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| Year of Study * | Third Year |
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| Semester when the Course Unit is delivered | Summer Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| DVO54 | prof. RNDr. Richard Dvorský, Ph.D. |
| Summary |
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| The course follows the "Experimental methods and tools for nanotechnology II" and focuses on the practical application of laboratory techniques selected physical characterization of nanostructures. |
| Learning Outcomes of the Course Unit |
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| Practical application of selected nanostructure diagnostics techniques. |
| Course Contents |
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LABORATORY PRAXIS
1. Introduction and security training
2. UV-VIS absorption spectral analysis
3. DRS - diffusion reflex spectroscopic analysis (Kubelka-Munk reflektance)
4. UV-VIS Absorption - Determination of the bandwidth of the non-polarized nanoparticle band
5. UV-VIS Absorption - Determination of nanoparticle size by applying the Brush equation
6. Measurement of photocatalytic efficiency of semiconducting nanoparticles by UV-VIS absorption in real time
7. FTIR - spectroscopic analysis
8. RS - Raman spectroscopic analysis
9. PL - PhotoLuminiscence Spectroscopic Analysis
10. ED - Electron diffraction
11. LDA - Laser diffraction analysis
12. Determination of statistical distribution of nanoparticles by DLS - Dynamic light scattering
13. Measurement of zeta-potential of nanoparticles by DLS - Dynamic light scattering
14. Activation analysis |
| Recommended or Required Reading |
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| Required Reading: |
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KITTEL, Charles. Introduction to Solid State Physics. 8th ed. John Wiley & Sons. c2005 ISBN: 0-471-41526-X.
AGRAWAL, Dinesh Chandra. Introduction to nanoscience and nanomaterials. Singapore: World Scientific, c2013. ISBN 978-981-4397-97-1.
MYHRA, Sverre a J. C. RIVIERE. Characterization of nanostructures. Boca Raton: CRC Press, c2013. ISBN 978-1-4398-5415-0.
MUSA, Sarhan M., ed. Nanoscale spectroscopy with applications. Boca Raton: CRC Press, c2014. ISBN 978-1-4665-6853-2. |
KITTEL, Charles. Úvod do fyziky pevných látek. Přeložil Miloš MATYÁŠ. Praha: Academia, 1985.
AGRAWAL, Dinesh Chandra. Introduction to nanoscience and nanomaterials. Singapore: World Scientific, c2013. ISBN 978-981-4397-97-1.
MYHRA, Sverre a J. C. RIVIERE. Characterization of nanostructures. Boca Raton: CRC Press, c2013. ISBN 978-1-4398-5415-0.
MUSA, Sarhan M., ed. Nanoscale spectroscopy with applications. Boca Raton: CRC Press, c2014. ISBN 978-1-4665-6853-2. |
| Recommended Reading: |
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LENG, Yang. Materials characterization: introduction to microscopic and spectroscopic methods. 2nd ed. Weinheim: Wiley-VCH, c2013. ISBN 978-3-527-33463-6.
GOLDENBERG, P. David. A Guide to SAXS Data Processing with the Utah SAXS Tools with Special Attention to Slit Corrections and Intensity Calibration. Department of Biology University of Utah, c2012.
SCHNABLEGGER, Heimo a SINGH, Y. The SAXS guide. Anton Paar GmbH, c2013. ISBN 180-120-13.
FULTZ, Brent a HOWE, James. Transmission Electron Microscopy and Diffractometry of Materials, Springer-Verlag Berlin, c2013. ISBN 978-3-642-29761-8. |
LENG, Yang. Materials characterization: introduction to microscopic and spectroscopic methods. 2nd ed. Weinheim: Wiley-VCH, c2013. ISBN 978-3-527-33463-6.
GOLDENBERG, P. David. A Guide to SAXS Data Processing with the Utah SAXS Tools with Special Attention to Slit Corrections and Intensity Calibration. Department of Biology University of Utah, c2012.
SCHNABLEGGER, Heimo a SINGH, Y. The SAXS guide. Anton Paar GmbH, c2013. ISBN 180-120-13.
FULTZ, Brent a HOWE, James. Transmission Electron Microscopy and Diffractometry of Materials, Springer-Verlag Berlin, c2013. ISBN 978-3-642-29761-8. |
| Planned learning activities and teaching methods |
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| Tutorials, Experimental work in labs |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Graded credit | Graded credit | 100 | 51 |