| Course Unit Code | 9360-0142/04 |
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| Number of ECTS Credits Allocated | 3 ECTS credits |
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| Type of Course Unit * | Choice-compulsory type B |
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| Level of Course Unit * | Second Cycle |
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| Year of Study * | Second Year |
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| Semester when the Course Unit is delivered | Summer Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| SIM75 | prof. Ing. Gražyna Simha Martynková, Ph.D. |
| Summary |
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| The subject is focused on experimental methods of characterization of nanomaterials and is linked with subjects Nanomaterials based on natural materials and Methods of structural and phase analysis. |
| Learning Outcomes of the Course Unit |
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| The knowledge in laboratory and analytical techniques for characterization of nanomaterials are main output of subject. |
| Course Contents |
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1. Introduction to laboratory practice - introduction to the subject matter and conditions of its completion. Safety at work in the laboratory. . Preparation of different types of samples for chemical and structural analysis.
3. Mechanical processing (crushing, grinding, friction and homogenization).
4. Evaluation of particulate materials - size and distribution.
5. Morphological characterization of powders - microscopy.
6. Modification of layered materials and exfoliation-delamination. organophilization.
7. Embedding nanowires into the composite matrix.
8. Evaluation of nanoparticles in composites.
9.Infrared spectroscopy - structural analysis.
10. Raman spectroscopy structural analysis.
11. X-ray diffraction analysis phase and structural evaluation. 12.Termogravimetric analysis of temperature and materials conversion.
13. Quantitative and qualitative analysis of data comparison from different analytical methods.
14. Molecular modeling of structures and interaction. |
| Recommended or Required Reading |
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| Required Reading: |
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YARIV S., CROSS H.: Organo-Clay Complexes and Interactions. New York, Basel, 2002, 688 p, ISBN 0-8247-0586-6.
Fine Particles, Synthesis, Characterization and Mechanism of Growth. Edited by. T. Sugimoto. Marcel Dekker, New York, 2000.
Nanostructure Science and Technology. Edited by Siengel, W., R., Hu, E., Roco, M., C. Kluwer Academic Publisher, London 1999. ISBN 0-7923-5854-6. |
WEISS Z., KUŽVART M.: Jílové minerály, jejich nanostruktura a vlastnosti. Praha: UK, Karolinum, 2005, 281 s. ISBN 80-246-0868-5.
ŠUCHA V.: Íly v geologických procesoch. Acta Geologica Universitatis Comenianae, 2001, 159 s., ISBN 80-223-1547-8.
YARIV S., CROSS H.: Organo-Clay Complexes and Interactions. New York, Basel, 2002, 688 p, ISBN 0-8247-0586-6.
Fine Particles, Synthesis, Characterization and Mechanism of Growth. Edited by. T. Sugimoto. Marcel Dekker, New York, 2000.
Nanostructure Science and Technology. Edited by Siengel, W., R., Hu, E., Roco, M., C. Kluwer Academic Publisher, London 1999. ISBN 0-7923-5854-6. |
| Recommended Reading: |
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Vermiculite: structural properties and examples of the use; Valášková, Marta, Simha Martynkova, G.: Clay minerals in nature-their characterization, modification and application, InTech, 209-238,2012.
Sneha Mohan Samuel Oluwatobi Oluwafemi Nandakumar Kalarikkal Sabu Thomas, eds.: Characterization of Nanomaterials, Woodhead Publishing, ISBN: 9780081019733. |
| Sneha Mohan, Samuel Oluwatobi, Oluwafemi Nandakumar, Kalarikkal Sabu Thomas, eds.: Characterization of Nanomaterials, Woodhead Publishing, ISBN: 9780081019733. |
| Planned learning activities and teaching methods |
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| Seminars, Tutorials, Experimental work in labs |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Graded credit | Graded credit | 100 | 51 |