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Terminated in academic year 2007/2008

Instrumental Methods of Analysis I

Type of study Bachelor
Language of instruction Czech
Code 546-0335/01
Abbreviation IMA I
Course title Instrumental Methods of Analysis I
Credits 9
Coordinating department Department of Environmental Engineering
Course coordinator doc. Mgr. Eva Pertile, Ph.D.

Subject syllabus

1. Determination problems. Basic notions. Processes data acquisition. Basic classification of analytical methods.
2. Basic units of concentration and calculations. Type of interaction. Chemical balances in analytical chemistry. Classification of analytical reaction.
3. Case of analyses – common tissue: exercise formulation and proposal; sampling, sample adjustment before analysis; separative and concentration steps; measurement; measurement interpretation and formulation of results analyses; activities proposal resulting from acquired dates.
4. Sampling, common sampling fundamentals. Standard operational procedure for sampling; system QA/QC.
5. Basic sampling characteristics for abiotic and biotic matrixs. Atmosphere sampling, including passive sampling.
6. Sampling drinking and surface waters; sediment sampling; sampling underground and outlet waters; sampling sludge from sewage disposal plant; sampling soil sphere.
7. Biotic matrixs sampling. Wastes sampling.
8. Sample adjustment before analysis. Analytical method NDRO. Destructive analytical methods: Samle solution and analysis, mineralization.
9. Separative and concentration steps: elimination interference with chemical methods (masking) and physical speparation. Separative methods: dividing according to axiom and according to experimental ordering. Extraction. Separation on ion exchanger. Influence separative of the process.
10. Classification of analytical results and techniques and formulation results of analyses. A ctivities proposal implicit from gained data. GLP. Chemometric principles.
11. Principles of qualitative analyses: classic system of dividing cation – hydrogen sulphide system, analytical anion classes. Next criteria at anion determination. Heteroatoms verification in organic matter.
12. View of basic analytical methods and their common property: method based on weighing, on measuring of volume. Gravimetric analysis: axioms, analytical usage. Basic steps of analyses: sample adjustment, removing, washinh process and filtration, drying, coagulation weighing,concentration calculation .
13. Quantitative chemical analysis. Volumetric analysis (volumetry): common procedure of determination, determination final point of titration, titration curve, calculation of sample content from titrating data. Types of volumetric determination and their application: acidobasic titration, coagulative titration, complex-forming agent titration, redox titration. Axioms, analytical usage.
14. Developments in analytical chemistry - mobile analytics.

Literature

PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3 .
CHANG R. Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Available from: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang.
GRANGER, B. New developments in analytical chemistry research. New York: Nova Publishers, 2015. Chemistry research and applications series. ISBN 1634634276 .
ANDRADE G., J. M. A. CARLOSENA ZUBIETA, M. P. GÓMEZ-CARRACEDO, M. Á. MAESTRO SAAVEDRA, M. C. PRIETO-BLANCO and R. M. SOTO-FERREIRO. Problems of instrumental analytical chemistry: a hands-on guide. New Jersey: World Scientific, 2017. Essential textbooks in chemistry. ISBN 978-1-78634-179-2 .

Advised literature

Trends in Environmental Analytical Chemistry [online]. 2018, 17-20(4). ISSN 2214-1588 . Dostupné z: https://www.sciencedirect.com/journal/trends-in-environmental-analytical-chemistry.
HANRAHAN, G. Key concepts in environmental chemistry. Burlington: Elsevier Science, 2011. ISBN 9780080961705 . Dostupné z: http://booksite.elsevier.com/samplechapters/9780123749932/Front_Matter.pdf.
AHUJA, S. Chemistry and water: the science behind sustaining the world's most crucial resource. Amsterdam: Elsevier, 2017. ISBN 978-0-12-809330-6 . Dostupné z: https://www.sciencedirect.com/science/book/9780128093306.
PETROZZI, S. Practical instrumental analysis: methods, quality assurance and laboratory management. Weinheim: Wiley-VCH, c2013. ISBN 978-3-527-32951-9.