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Terminated in academic year 2008/2009

Instrumental Methods of Analysis

Type of study Bachelor
Language of instruction Czech
Code 546-0354/02
Abbreviation IMA
Course title Instrumental Methods of Analysis
Credits 6
Coordinating department Department of Environmental Engineering
Course coordinator doc. Mgr. Eva Pertile, Ph.D.

Subject syllabus

1. Problems delimitation. Basic concepts. Processes obtaining information. Analytical methods absolute and comparative. Calibration methods. Developments in instrumentation methods of analyses.
2. - 3. Results classification of analyses and way their explication. Statistical interpretation of analytical results. Referential material, circular test. Principles of chemometric accesses and methods. Testing of metrological results properties.
4. Fundamental principles of electroanalytical methods and their classification. Theoretic principles.
5. Electroanalytical methods: methods based on measuring of potential (equilibrium potentiometry, potentiometric titrations). Axioms, instrumentation, utilization, advantages and disavantages.
6. Electroanalytical methods: methods based on current (voltammetry and polarography, coulometry, electrogravimetry) and conductivity (conductometry). Axioms, instrumentation, utilization, advantages and disavantages.
7. Optical analytical methods: theoretic principles. Optical spectral apparatus. Methods without exchange of energy (refractometry, polarimetry, nephelometry). Axioms, instrumentation, utilization, advantages and disavantages.
8. - 9. Emissive atomic spectral frequency bands. Flame photometer photometry. Atomic absorptive spectrometric: UV/Vis spectrometric, luminescent analysis. Principles theory, instrumentation, qualitative and quantitative aspects, application, analytical utilization. Automatic analyzers with optical detection: FIA, CFA.
10. Infra - red spectrometric - method axiom, instrumentation, analytical utilization. Raman spectra - method axiom , analytical utilization.
11. Separative and concentration steps: theory. Separative methods:classification according to axiom and according to experimental ordering, operation separative of the process. Extraction.
12. Diaphragm separation. Mass spectrometry. Bases theory, instrumentation, qualitative and quantitative aspects, application.
13. Chromatographic methods. Planar chromatography: Chromatography on thin layer, bases theory, instrumentation, qualitative and quantitative aspects, application.
11. Column chromatography: Liquid chromatography. Gas chromatography. Theory, bases instrumentation, qualitative and quantitative characteristics, analytical utilization.
14. Electromigration methods: theory, zonal and capillary electrophoresis, isotachophoresis. Bases instrumentation, qualitative and quantitative characteristics, analytical utilization.

Literature

CHANG R.: Chemistry. 10th Edition. McGraw-Hill: New York, 2010. 1170 p. Dostupné z: https://archive.org/details/Chemistry_10th_Edition_Raymond_Chang
PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3

Advised literature

ROUESSAC Francis and ROUESSAC, Annick: Chemical Analysis Modern Instrumentation Methods and Techniques. March 2007. 600 pp. ISBN: 978-0-470-85903-2 
NOLLET M., L., Chromatographic Analysis of the Environment, Chromatographic Science Series, Volume 93, 1297 s. 2006, ISBN 0-8247-2629-4