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Ukončeno v akademickém roce 2023/2024

Instrumental Methods of Chemical Analysis

Type of study Doctoral
Language of instruction English
Code 546-0940/03
Abbreviation IMCH
Course title Instrumental Methods of Chemical Analysis
Credits 10
Coordinating department Department of Environmental Engineering
Course coordinator doc. Mgr. Eva Pertile, Ph.D.

Osnova předmětu

Information retrieval processes. Automation of measurement and data collection, continuous measurement of chemical characteristics in treatment.
Evaluation of analytical results and procedures, expression of chemical analysis results. Statistical processing of results. Proposal of activities resulting from the obtained data. GLP principles.
Methods of control of technological processes (development of analytical methods, the superstructure of analytical chemistry with a focus on industrial processes). Development and standardization of analytical methods.
Operating procedures for sampling; QA / QC system. Sample preparation before analysis.
Absolute and comparative analytical methods. Rapid analytical methods - screening. Calibration methods. Portable devices for the analysis of materials in landfills and in the field, parameters for their selection and evaluation.
Selected electroanalytical methods applied in the analysis of mineral resources, treatment products and processing of environmental material. Sample preparation, application.
Separation methods applied in the analysis of mineral raw materials, products of treatment and processing of environmental material - theoretical foundations and practical possibilities.
Optical methods applied in the analysis of mineral resources, products of treatment and processing of environmental material. Sample preparation, application.
Scanning probe surface analysis (STM, AFM, SNOM); photon probe (PES, XPS, UPS, LAMMS, etc.); electron probe (EPXMA, SEM, combined AEM, AES, etc.), ion probe (RBS, ISS, SIMS, etc.); pole probe (FIM, etc.).
New trends in instrumental methods with application in conditioning. Coupling techniques GC-MS, LC-MS, CE-MS, GC / LC-ICP-MS, speciation analysis, LC / GC-IR, LC-NMR.

Povinná literatura

KENKEL J.: Analytical chemistry for technicians. 4th Edition, CRC Press, Boca Raton, 2013, 1-537.
MILLER James, Jane C MILLER. Statistics and Chemometrics for Analytical Chemistry. Pearson Education Limited, 2018. ISBN: 1292186712 .
PERTILE, E. Instrumental Methods of Analysis. Ostrava: Vysoká škola báňská - Technická univerzita Ostrava, 2017. ISBN 978-80-248-4124-3 .
HARVEY T. D. Analytical Chemistry 2.1. Electronic Versions. 2016 http://dpuadweb.depauw.edu/harvey_web/eTextProject/AC2.1Files/AnalChem2.1.pdf.

Doporučená literatura

FIELD L. D., STERNHELL S., KALMAN J. R. Organic Structures from Spectra. New York, United States: John Wiley & Sons Inc. 2013. ISBN 978-1-118-32549-0 .
PRETSCH E., BÜHLMANN P., BADERTSCHER M. Structure Determination of Organic Compounds : Tables of Spectral Data. Berlin, Germany: Springer-Verlag Berlin and Heidelberg GmbH & Co. KG. 2009. ISBN13 9783540938095 .
WEINER E.R. Applications of aquatic chemistry: a practical guide. 3rd edition, CRC Press, Boca Raton, 2012, 1-618.
Analytical chemistry: a modern approach to analytical science. 2nd ed. Editor J.-M MERMET, editor M. OTTO, editor M. VALCÁRCEL. Weinheim: Wiley-VCH, c2004. ISBN 3527305904 .