Terminated in academic year 2011/2012

Solid Phase Structure

Type of study	Bachelor
Language of instruction	Czech
Code	617-0411/01
Abbreviation	SPF
Course title	Solid Phase Structure
Credits	4
Coordinating department	Department of Chemistry
Course coordinator	prof. Ing. Boleslav Taraba, CSc.

Subject syllabus

1) The textural properties of solids. Basic parameters of texture, density
solids, porosity
2) The theory of adsorption on solids, adsorption isotherm, Brunnauer
classification
3) Experimental procedures for determining the textural parameters
4) Types of adsorption ISOTERM, the theory of monomolecular Langmuir adsorption isotherm
5) The theory of multilayer adsorption (BET)
6) Adsorption in micropores, Polanyi potential, Dubinin-Raduškevič isotherm, calculations
7) Adsorption in mesopores, capillary condensation, Kelvin equation
8) Adsorption in a flow-through arrangement
9) The adsorption of gas mixtures, sorption of the liquid medium
10) The assessment of substances in terms of texture fractal geometry
11) The flow of gases and liquids porous environment, viscous flow, Knudsen diffusion, specific permeability
12) Experimental methods, apparatus, evaluation, reproducibility

Literature

1) Silverstein,R.M., Bassler,G.C., Morril,T.C.: Spectrometric Identification of Organic Compounds. 5th edition, J.Wiley & Sons, New York 1991
2) George,W.O., McIntyre,P.S.: Infrared Spectroscopy - Analytical Chemistry by Open Learning, John Wiley & Sons, New York, 1990
3) Kalous,V.: Jak moderní chemie zkoumá strukturu molekul, SNTL, Praha, 1987
4) J.Zýka a kol.: Nové směry v analytické chemii, Sv 4, SNTL Praha, 1988
5) Ponec,V., Knor,Z., Černý,S.: Adsorpce na tuhých látkách, Praha SNTL, 1968
6) Gregg,S.J., Sing,K.S.W.: Adsorption, Surface Area and Porosity (2nd edition), Academic Pess, London, 1982
7) Taraba,B.: Chemická struktura pevné fáze, Učební texty OU, PřF, Ostravská univerzita 1995.
8) R.Ch.Bansal, J.B.Donnet, F.Stoeckli: Active Carbon, Marcel Dekker Inc., New York, 1988.
9) M.A.Wright, K.R.Palmer: Research into Structural Carbons, SIU, Carbondale, 1994

Advised literature

No advised literature has been specified for this subject.

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