Lectures
1. Utilization and division of analytical chemistry, basic units, statistical treatment of analytical data.
2. Selection and characteristics of analytical methods. Sampling, pre-treatment of samples.
3. Volumetric analysis. Acid-base titration.
4. Complexometric titration, oxidation-reduction titration.
5. Precipitation titration and gravimetry.
6. Models of atom, spectral analysis, atomic emission spectrometry.
7. X-ray spectra, X-ray fluorescence spectrometry.
8. Molecular spectra, UV-VIS absorption spectrometry.
9. Vibration of molecules, infrared spectra.
10. Electrochemical potential, electrodes, potentiometry.
11. Electrolysis, polarography.
12. Conductivity, conductometry.
13. Separation principles, gas and liquid chromatography.
14. Migration of ions in electric field, capillary isotachophoresis and electrophoresis.
Laboratory exercises
• Basic analytical operations
• Calibration of volumetric vessels
• Manganometric determination of iron in ore
• Alkalimetric determination of molar concentration of phosphoric acid
• Gravimetric determination of loss of limestone
• Alkalimetric determination of carbonate content in limestone
• Chelatometric determination of calcium and magnesisum
• Argentometric determination of chloride
• Mercurymetric determination of chloride
• Gravimetric determination of iron
• Iodometric determination of iodate
• Gravimetric determination of nickel
• Chelatometric determination of bismuth and lead
• Polarographic study (determination of cadmium, nickel and zinc)
• Spectrophotometric study (determination of manganem and chromium in the VIS region)
• Potenciometric determination of pH
• Potenciometric determination of chromium and vanadium in steel
• Determination of chloride by ion selective electrode
• Determination of cadmium and lead by atomic absorption spectrometry
• Conductometric determination of specific electrolytic conductivity of water
• Validation of a method for determination of chromium in water by VIS spectrophotometry
• Determination of elements in coal by X-ray fluorescence analysis
1. Utilization and division of analytical chemistry, basic units, statistical treatment of analytical data.
2. Selection and characteristics of analytical methods. Sampling, pre-treatment of samples.
3. Volumetric analysis. Acid-base titration.
4. Complexometric titration, oxidation-reduction titration.
5. Precipitation titration and gravimetry.
6. Models of atom, spectral analysis, atomic emission spectrometry.
7. X-ray spectra, X-ray fluorescence spectrometry.
8. Molecular spectra, UV-VIS absorption spectrometry.
9. Vibration of molecules, infrared spectra.
10. Electrochemical potential, electrodes, potentiometry.
11. Electrolysis, polarography.
12. Conductivity, conductometry.
13. Separation principles, gas and liquid chromatography.
14. Migration of ions in electric field, capillary isotachophoresis and electrophoresis.
Laboratory exercises
• Basic analytical operations
• Calibration of volumetric vessels
• Manganometric determination of iron in ore
• Alkalimetric determination of molar concentration of phosphoric acid
• Gravimetric determination of loss of limestone
• Alkalimetric determination of carbonate content in limestone
• Chelatometric determination of calcium and magnesisum
• Argentometric determination of chloride
• Mercurymetric determination of chloride
• Gravimetric determination of iron
• Iodometric determination of iodate
• Gravimetric determination of nickel
• Chelatometric determination of bismuth and lead
• Polarographic study (determination of cadmium, nickel and zinc)
• Spectrophotometric study (determination of manganem and chromium in the VIS region)
• Potenciometric determination of pH
• Potenciometric determination of chromium and vanadium in steel
• Determination of chloride by ion selective electrode
• Determination of cadmium and lead by atomic absorption spectrometry
• Conductometric determination of specific electrolytic conductivity of water
• Validation of a method for determination of chromium in water by VIS spectrophotometry
• Determination of elements in coal by X-ray fluorescence analysis