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Terminated in academic year 2009/2010

Properties of Ceramic Materials II

Type of study Master
Language of instruction Czech
Code 635-0079/01
Abbreviation VKM II
Course title Properties of Ceramic Materials II
Credits 5
Coordinating department Department of Thermal Engineering
Course coordinator doc. Ing. Václava Tomková, CSc.

Subject syllabus

Lectures:
1 Gravimetric procedure in chemical analysis, principle.
2 Volumetric analysis - Neutralization, Chelatometry. The indicators in
volumetric analysis, examples.
3 Principle of spectral separation methods and chemical analysis. Absorption spectral
analysis, Lambert - Beer law. Colorimetry, photometry, spectrophotometry.
4 Emission spectral analysis. X-ray fluorescence analysis.
5 Overview of methods of phase analysis.
6 DTA, TG, dilatometry and thermo-mechanical analysis. Simultaneous thermal analysis
applications.
7 Principle of DSC calorimetry.
8 Calvets - Tian's equation in calorimetry applications. The basic methodology for
calorimetric measurements.
9 X-ray diffraction, Bragg equation, applications. X-ray, formation, monochromatization, utilization.
10 X-ray diffraction phase analysis - identification one substance. X-ray procedure phase
analysis of mixtures of minerals.
11 X-ray microanalysis, the principle use
12 Principles and applications of the TEM imaging.
13 Principles, and applications of SEM imaging (REM).

Seminars:
1 Preparation of solutions for chemical analysis. Expressing the composition of
standard solutions, determine the titre. Decomposition of samples for chemical
analysis, storage solution.
2 Determination of SiO2 + non decomposable share R2O3 determination, determination
of loss on drying and annealing.
3 Volumetric determination of CaO and MgO.
4 Photometric determination of Fe2O3.
5 DTA - evaluation of measurement applications. TG - analysis of data usage.
6 X-ray diffraction phase analysis..

Literature

1.KALOUS, V. Metody chemického výzkumu. Praha : SNTL, 1987. 430 s.
2.ŠESTÁK, J. Měření termofyzikálních vlastností pevných látek. Praha :
Academia, 1982. 345 s.
3.KLIKA, Z., PRAUS, P. Analytická chemie I. Ostrava : VŠB-TU, 2002. 172 s.

Advised literature

No advised literature has been specified for this subject.