Skip to main content
Skip header
Terminated in academic year 2018/2019

X-ray Diffraction Analysis

Type of study Follow-up Master
Language of instruction Czech
Code 9360-0011/01
Abbreviation RDA
Course title X-ray Diffraction Analysis
Credits 6
Coordinating department CNT - Nanotechnology Centre
Course coordinator doc. Mgr. Kateřina Mamulová Kutláková, Ph.D.

Subject syllabus

Content
1. Introduction- history, basic terms (definition of crystal, lattice types, Miller's indexes, crystallographic systems, minimal symmetry rules, reciprocal lattice).
2. Point symmetry, stereographic projection.
3. Group theory, crystallographic group of symmetry, symbols.
4. Matrix representation of symmetry operations.
5. Space group of symmetry; symbols, graphical illustration.
6. Crystallochemistry, crystallization processes, types of structure defects, crystal structure and chemical bond.
7. X-ray; principle, formation, forms, properties, registration, interaction with matter.
8. Diffraction of X-rays; Laue and Bragg equations; structural factor F (hkl).
9. X-ray diffraction methods, classification based on Ewald's scheme, Laue, Debye Scherrer, powder methods.
10. Powder diffractometers, indexation of powder patterns records, focusing methods, practical applications of powder methods.
11. Single crystal techniques; Weissenberg and precession method, types of diffractometers, complete X-ray analysis of crystal compounds.

Literature

Frank H. Chung and Deane K. Smith: Industrial Applications of X-Ray Diffraction, Taylor & Francis Group, 2000. ISBN: 0-8247-1992-1

Advised literature

BISH, D. L., POST, J. E.: Eds. Modern Powder Diffraction, Reviews in
Miner.Vol. 20, Washington, D.C., 1989.
BLOSS, F. D: Crystallography and Crystal, Chemistry.- Holt, Rinehart and
Winston, Inc., 1971.