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Methods of organic analysis for characterization of nanostructured materials

Type of study Doctoral
Language of instruction English
Code 9360-0207/02
Abbreviation MOA
Course title Methods of organic analysis for characterization of nanostructured materials
Credits 10
Coordinating department CNT - Nanotechnology Centre
Course coordinator prof. Ing. Daniela Plachá, Ph.D.

Subject syllabus

Chromatographic methods, mass spectrometry.
Coupling of chromatographic methods with mass spectrometry, applications.
Spectroscopic methods for organic analysis, IR and Raman spectroscopy, applications.
Nuclear magnetic resonance and electron paramagnetic resonance, aplications.
Evaluation of chromatographic results.
Evaluation of mass spectra.
Basic principles and procedures for evaluation of IR spectra.
Basic principles and procedures for evaluation of Raman spectra.
Basic principles and procedures for evaluation of NMR spectra.
Basic principles and procedures for evaluation of EPR (ESR) spectra.
Preparation and development of analytical method for organic analysis.
Validation of method, measurement uncertainety.
Basic of Good laboratory Practise (GLP) and Quality Management in analytical laboratory.

Literature

H. J. Hübschmann, Handbook of GC/MS (Sec. Ed.), Wiley-VCH Verlag GmbH & Co., KGaA, Weinheim 2008. ISBN 978-3-527-31427-0 .
M. C. McMaster, LC/MS, John Wiley&Sons, New York 2005. ISBN 978-047-16553-12 .
G. Gauglitz, T. Vo-Dinh, Handbook of Spectroscopy, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim 2005. ISBN 978-3-527-29782-5 .
J. D. Winefordner, Sample Preparation Techniques in Analytical Chemistry, Volume 162, John Wiley & Sons, Inc. 2003. ISBN 0-471-32845-6 .

Advised literature

M. C. Mc Master, GC/MS (Sec. Ed.), John Wiley & Sons, Inc. Hoboken, NJ, USA 2007. ISBN 978-047-010163-6 .
S. Wartewig, IR and Raman Spectroscopy: Fundamental Processing, VCH Verlag GmbH & Co. KGaA, Weinheim 2003. ISBN 3-527-30245-X .
R. G. Brereton, Applied Chemometrics for Scientists, John Wiley & Sons, New York 2007. ISBN 9780470016862 .


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