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Nanomaterials on the phyllosilicates base

Type of study Follow-up Master
Language of instruction Czech
Code 9360-0145/03
Abbreviation NBVS
Course title Nanomaterials on the phyllosilicates base
Credits 3
Coordinating department CNT - Nanotechnology Centre
Course coordinator prof. Ing. Gražyna Simha Martynková, Ph.D.

Subject syllabus

1. Structure and crystal chemistry of silicates.
3. Layer charge, cation exchange in the interlayer, exfoliation, delamination,
intercalation.
4. Layered silicates and water in the interlayer space. Hydratation, dehydratatiion
and rehydratation.
5. Serpentine-kaolinite group. Structural ordering of kaolinites. Thermal change.
6. Halloysite.
7. Kaolinite and halloysite as clay nanofillers to polymers.
8. Talc-pyrophyllite group. Structure and modification for practical use.
9. Smectites. Cations exchange, modifications procedures.
10. Smectites as nanomaterials with specific properties.
11. Vermiculites. Thermal coversion of structure. Influence of acids on structure.
12. Vermiculite intercalation with metal compounds and their characteristics.
13. Organovermiculites. Preparation and characterization.
14. Clay minerals-polymers nanocomposites.

Laboratory exercises every 2 week.
1. Introduction, the content of laboratory exercises and requirements for obtaining credit, safety of work.
2. Preparation of clay fractions by grinding and sedimentation.
3. Preparation of monoionic form of silicate.
4. Preparation of organophilic forms of silicates.
5. Embedding the nanofiller into the polymer matrix.
6. Evaluation by analytical methods of the prepared nanocomposite.

Literature

MARTIN, R.T. (Charman), BAILEY, S.W., EBERL, D.D., FANNING, D.S., GUGGENHEIM, S., KODAMA, H., PEVEAR, D.R., ŚRODOŃ, J. a WICKS, F. J. 1991. Report of The Clay Minerals Society Nomenclature Committee: Revised Classification of Clay Materials. Clays Clay Miner., 39, 333-335.
VALÁŠKOVÁ, M., SIMHA MARTYNKOVÁ, G.: Vermiculite: structural properties and examples of the use. In: Clay Minerals in Nature, their Characterization, Modification and Application (M. Valášková and G. Simha Martynková, Eds.), InTech 2012, 209-238, ISBN 978-953-51-0738-5.

Advised literature

G. Simha Martynková, M. Valášková: Vermiculite in nanocomposites: In Encyclopedia of Nanoscience and Nanotechnology, 2nd Edition (H.S. Nalwa, editor), ASP 2011, Vol. 25, 119-145, ISBN: 1-58883-190-6.
Handbook of Clay Science Edited by F. Bergaya, B.K.G. Theng and G. Lagaly
Developments in Clay Science, Vol. 1, 2006 Elsevier Ltd., pp.1224, ISBN-10 0-08-044183-1