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Laboratory Practice of Nanonaterials Preparation

Type of study Bachelor
Language of instruction Czech
Code 9360-0185/01
Abbreviation LCPN
Course title Laboratory Practice of Nanonaterials Preparation
Credits 3
Coordinating department CNT - Nanotechnology Centre
Course coordinator Ing. Karla Čech Barabaszová, Ph.D. Paed.IGIP

Subject syllabus

1. Introductory tutorials. Introducing students to the lab, organizing laboratory exercises, safety and hygiene in laboratory work. Obligatory legal information to students about individual tasks, used chemicals and possible risks. Compilation of mandatory training documents.
Students work independently on the realization of laboratory tasks devoted to targeted preparation of nanostructured materials (see section 3-13). They use instrumentation, chemical reactants and chemical aids as specified in the protocol.
2. Ultrasonic synthesis of nanoparticles MgO.
3. Mechanochemical synthesis of CuO.
4. Preparation of Al2O3 particles by hydrolysis of AlCl3.
5. Solvothermal synthesis of ZnS nanoparticles.
6. Preparation of ZnO by the precipitation method.
7. Preparation of Ag nanoparticles by reaction with saccharides.
8. Preparation of CuO by microwave decomposition.
9. Preparation of magnetite by chemical precipitation reaction in liquids.
10. Preparation of ZnO nanoparticles by hydrothermal synthesis.
11. Roses - preparation of nanoparticles Ag.
12. Synthesis of CeO2 by precipitation from aqueous solution.
13. Chemical vapor deposition - preparation of 1 dimensional nanostructured materials.
14. Credit week. Replacement term The term is made by students who have missed the semester.

Literature

SUGIMOTO, Tadao, ed. Fine Particles, Synthesis, Characterization and Mechanism of Growth. Marcel Dekker, New York, 2000. ISBN 0842700015 .
HOSOKAWA, Masuo, NAITO, Makio, YOKOYAMA, Toyokazu and Kiyoshi NOGI. Nanoparticle Technology Handbook. Elsevier, 2017. ISBN 9780444563682 .
BAUERLEIN, Edmund et. al, ed. Handbook of Biomineralization: Biological Aspects and Structure Formation. Wiley-VCH, 2009, ISBN 3527318054.4.
RAO, C.N.R, ed. The Chemistry of Nanomaterials, Synthesis, Properties and Applications, Willey-VCH Weinheim, 2008. ISBN 3527306862.

Advised literature

RAI Mahendra and Clemens POSTEN. Green Biosynthesis of Nanoparticles - Mechanisms and Applications. CABI Publishing 2013, ISBN 9781780642239.
Naito, Moto et. al, Nanoparticle Technology Handbook. Elsevier, 2017. ISBN 9780444563682 .
Nalwa H. S., editor. Encyclopedia of Nanoscience and Nanotechnology. Vol. 1-4. American Scientific Publisher, 2004. ISBN 1-58883-056-1 .