| Course Unit Code | 9360-0122/03 |
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| Number of ECTS Credits Allocated | 3 ECTS credits |
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| Type of Course Unit * | Compulsory |
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| Level of Course Unit * | First Cycle |
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| Year of Study * | Second Year |
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| Semester when the Course Unit is delivered | Summer Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| TOM24 | doc. Ing. Vladimír Tomášek, CSc. |
| OTO30 | RNDr. Hana Otoupalíková |
| MIK39 | Ing. Barbora Thomasová, Ph.D. |
| Summary |
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| The subject give a view of methods of chemical analysis of materials. Attention will be particularly devoted, besides the common fundamentals of analytical chemistry and basic methods, on instrumental methods. Students will be acquainted with the basics of spectroscopic, electrochemical and separation methods. Attention will be devoted on applications for chemical composition analysis of materials. |
| Learning Outcomes of the Course Unit |
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| The goal is to acquire a view of basic methods of chemical analysis. |
| Course Contents |
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1. Introduction, sampling, sample preparation.
2. Gravimetric analysis. Required laboratory equipment, overview of gravimetric methods, application.
3. Volumetric analysis. Required laboratory equipment, overview of volumetric methods, application.
4. Introduction to electrochemical methods. Conductometry, potentiometry, theoretical foundations. Using for direct measurement and for determination of end of titration.
5. Voltammetry, principle. Polarography, voltammetry on solid electrodes. Instrumentation, applications.
6. Electrogravimetry and coulometry, principle. Instrumentation, applications.
7. Introduction to separation methods, theoretical foundations. Extraction, distillation, membrane separation.
8. Introduction to spectral analysis, theoretical foundations. Overview of spectral methods.
9. X-Ray spectral analysis, theoretical foundations, methods of excitation of X-rays. X-Ray fluorescence spectrometry (XRF), construction of spectrometers, examples of use.
10. Atomic emission spectrometry (AES), principle. Spark and arc excitation and excitation in glowing discharge. AES with inductively coupled plasma (ICP).
Instrumentation, application.
11. Atomic absorption spectrometry, principle. Flame and electrothermal atomization, hydride generation, cold vapor mercury. Instrumentation, application.
12. Molecular absorption spectrometry, principle. Interaction of electromagnetic radiation with molecules. Spectrometry in visible and near ultraviolet range. Instrumentation, application.
13. Mass spectrometry. Radio-analytical methods. Electron spectrometry (Auger electrons, X-ray photoelectrons-XPS), secondary ion mass spectrometry. Instrumentation, application. |
| Recommended or Required Reading |
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| Required Reading: |
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KENKEL, John. Analytical Chemistry for Technicians. Boca Raton: CRC Press, 2002. ISBN 978-1-4398-8105-7.
MERMET, Jean-Michel, OTTO, M., VALCÁRCEL, M. Analytical chemistry, a modern approach to analytical science. Wiley - VCH, 2004. ISBN 3-527-30590-4 |
HOLZBECHER, Záviš a Jaroslav CHURÁČEK. Analytická chemie. Praha: SNTL, 1987.
KENKEL, John. Analytical Chemistry for Technicians. Boca Raton: CRC Press, 2002. ISBN 978-1-4398-8105-7. |
| Recommended Reading: |
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| KELLNER, R., MERMET, M., OTTO, M. and WIDMER, H. M. Analytical Chemistry. Weinheim: Wiley-VCH, 1998. ISBN 3-527-28881-3 |
ZÝKA, Jaroslav a kolektiv. Analytická příručka. 1. a 2. díl. Praha: SNTL, 1988.
GARAJ, Juraj a kolektiv. Fyzikálne a fyzikálnochemické analytické metódy. Bratislava: ALFA, 1977.
ŠTULÍK, Karel a kolektiv. Analytické separační metody. Praha: Karolinum, 2004. ISBN 80-246-0852-9.
KELLNER, R., MERMET, M., OTTO, M. and WIDMER, H. M. Analytical Chemistry. Weinheim: Wiley-VCH, 1998. ISBN 3-527-28881-3.
PRAUS, Petr, Václav DOMBEK a Zdeněk KLIKA. Základy analytické chemie. Ostrava: ES VŠB-TU, 2000.
KLIKA, Zdeněk. Z a Petr PRAUS. Analytická chemie I. Ostrava: ES VŠB-TU, 2002.
POPL, Milan a kolektiv. Instrumentální analýza. Praha: SNTL, 1986.
SOMMER, Lumír. Základy analytické chemie I. Brno: VUTIUM, 1998. ISBN 80-214-1300-X.
SOMMER, Lumír. a kolektiv. Základy analytické chemie II. Brno: VUTIUM, 2000. ISBN 80-214-1742-0.
TOMÁŠEK, Vladimír, Viktor KANICKÝ a kol. Zásady a možnosti analýzy anorganických látek. Český Těšín: 2THETA, 2014. ISBN 978-80-260-7238-6. |
| Planned learning activities and teaching methods |
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| Lectures |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Examination | Examination | 100 | 51 |