| Course Unit Code | 617-3016/01 |
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| Number of ECTS Credits Allocated | 5 ECTS credits |
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| Type of Course Unit * | Compulsory |
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| Level of Course Unit * | Second Cycle |
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| Year of Study * | Second Year |
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| Semester when the Course Unit is delivered | Winter Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| RIT37 | doc. Ing. Michal Ritz, Ph.D. |
| PAV57 | Ing. Jiří Pavlovský, Ph.D. |
| Summary |
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| Subject deals with structure of chemical compounds description from either theoretic (simulation and theoretic calculations) or practical (intensification of spectral and separation methods of instrumental structural analysis) point of view. |
| Learning Outcomes of the Course Unit |
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Objective of the course - aims of the course unit: To teach students the basis of evaluation of the results of selected methods (XRD, NMR, vibration spectroscopy, MS, ...) for identification of chemical compounds and substances.
Acquired knowledge: theoretical and practical knowledge of the spectra of selected analytical methods for the identification of chemical compounds and substances.
Acquired skills: ability to evaluate the spectra of selected analytical methods for the identification of chemical compounds and substances. |
| Course Contents |
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-Nuclear magnetic resonance: principle of the method, instrumentation, measurement techniques, NMR spectra and their interpretation
Mass spectroscopy: method principle, instrumentation, measurement techniques, MS spectra and their interpretation
-Rentgen diffraction analysis: interpretation of XRD records for identification of chemical compounds a substances
-Vibration spectroscopy: Interpretation of vibrational spectra for identification of chemical compounds a substances
-Nuclear Magnetic Resonance: Interpretation of NMR spectra for identification of chemical compounds a substances
Mass Spectroscopy: The interpretation of mass spectra for identification of chemical compounds a substances
-Luminiscent spectroscopy: interpretation of luminescence spectra for identification of chemical compounds a substances
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| Recommended or Required Reading |
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| Required Reading: |
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FIELD, L. D., STERNHELL, S., and KALMAN, J.R. Organic Structures from Spectra, 4th Edition. Chichester: John Wiley & Sons Ltd, 2008. ISBN 978-0-470-31926-0.
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SMRČKOVÁ-VOLTROVÁ, S. a BÖHM, S. Strukturní analýza organických sloučenin. Praha: VŠCHT, 1995. ISBN: 80-7080-235-9.
HORÁK, M. a VÍTEK, A. Zpracování a interpretace vibračních spekter. Praha: SNTL, 1980.
HORÁK, M. a PAPOUŠEK, D. Infračervená spektra a struktura molekul. Praha: Academia, 1976.
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| Recommended Reading: |
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COLOMBINI, M.P. and MODUGNO, F. Organic mass spectrometry in art and archeology. Chichester: Willey, 2009. ISBN: 978-0-470-51703-1.
CLERC, T. Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods (Studies in analytical chemistry). Elsevier Science Ltd, 1981. ISBN 13 9780444997487. |
GOLJER, I. a LIPTAJ, T. Nové metódy FT NMR spektroskopie kvapalín. Bratislava: Veda, 1986.
ČÁSLAVSKÝ, J. Hmotnostní spektrometrie a životní prostředí. Brno: Vitium, 2014. ISBN: 9778-80-214-5103-2
PRAUS, P. a VONTOROVÁ, J. Analytická chemie II. Ostrava: VŠB – technická univerzita Ostrava, 2015. ISBN 978-80-248-3734-5 |
| Planned learning activities and teaching methods |
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| Lectures, Tutorials, Other activities |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Credit and Examination | Credit and Examination | 100 (100) | 51 |
| Credit | Credit | 45 | 20 |
| Examination | Examination | 55 | 6 |