| Course Unit Code | 637-0003/01 |
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| Number of ECTS Credits Allocated | 2 ECTS credits |
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| Type of Course Unit * | Optional |
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| Level of Course Unit * | Second Cycle |
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| Year of Study * | |
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| Semester when the Course Unit is delivered | Winter, Summer Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| MAL37 | doc. Ing. Jitka Malcharcziková, Ph.D. |
| Summary |
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| Learning Outcomes of the Course Unit |
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- student will be able to describe principles of spectrometry
- student will be able to characterize OES and ED-XRF spectrometry methods
- student will be able to prepare samples for analysis, perform measurements and evaluate the obtained data
- student will be able to assess the suitability of using the OES and ED-XRF method
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| Course Contents |
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Introduction to spectrometry, non-destructive chemical analysis
Basic principles of optical emission spectrometry
Basic principles of X-ray fluorescence spectrometry
Preparation of samples for measurement
Chemical analysis by OES method
Chemical analysis by ED-XRF method
Determination of chemical composition of selected metals and their alloys
Determination of chemical composition of metallic waste
Determination of selected elements in non-metallic materials (soils)
Heavy metals in the environment
Evaluation and processing of obtained results
Assessment of the suitability of using the OES and ED-XRF method
Advantages and disadvantages of using the OES and ED-XRF method for selected types of metallic materials
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| Recommended or Required Reading |
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| Required Reading: |
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JOOSTEN, H. G., et al. Atomic Emission Spectrometry: AES - Spark, Arc, Laser Excitation. De Gruyter, 2020, 315 s. ISBN 9783110527681.
THIELE, G. Chemical Analysis of metal samples using Optical Emission Spectroscopy [online]. 2019. Dostupné z https://www.expertevents.com.au/wp-content/uploads/20191018-Glen-Thiele-Chemical-analysis-of-metal-samples-using-OES-copy-for-distribution.pdf.
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MALCHARCZIKOVÁ, J. Recyklace materiálů. 2019, E-book, VŠB-TUO, Ostrava, 201 s.
JOOSTEN, H. G., et al. Atomic Emission Spectrometry: AES - Spark, Arc, Laser Excitation. De Gruyter, 2020, 315 s. ISBN 9783110527681.
THIELE, G. Chemical Analysis of metal samples using Optical Emission Spectroscopy [online]. 2019. Dostupné z https://www.expertevents.com.au/wp-content/uploads/20191018-Glen-Thiele-Chemical-analysis-of-metal-samples-using-OES-copy-for-distribution.pdf.
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| Recommended Reading: |
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GILMORE, Gordon. Practical gamma-ray spectrometry. 2nd ed. Chichester: Wiley, c2008, 387 s. ISBN 978-0-470-86196-7.
NORDBERG, G. Handbook on the toxicology of metals. Burlington: Elsevier/Academic Press, 2007. ISBN 978-0-12-369413-3
b |
BENCKO, V., M. CIKRT a J. LENER. Toxické kovy v životním a pracovním prostředí člověka. Vyd. 2. Praha: Grada, 1995. ISBN 80-7169-150-X.
ČÁSLAVSKÝ, J. Hmotnostní spektrometrie a životní prostředí: Mass spectrometry and the environment. Brno: VUTIUM, 2014. ISBN 978-80-214-5103-2.
HÄBERLE, G. D. Technika životního prostředí pro školu i praxi. Praha: Europa-Sobotáles, 2003, 336 s. ISBN 80-86706-05-2.
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| Planned learning activities and teaching methods |
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| Seminars, Tutorials |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Graded credit | Graded credit | 100 | 51 |