| Course Unit Code | 651-2057/01 |
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| Number of ECTS Credits Allocated | 5 ECTS credits |
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| Type of Course Unit * | Compulsory |
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| Level of Course Unit * | First Cycle |
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| Year of Study * | Second Year |
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| Semester when the Course Unit is delivered | Summer Semester |
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| Mode of Delivery | Face-to-face |
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| Language of Instruction | Czech |
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| Prerequisites and Co-Requisites | Course succeeds to compulsory courses of previous semester |
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| Name of Lecturer(s) | Personal ID | Name |
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| OTY0005 | prof. RNDr. Michal Otyepka, Ph.D. |
| Summary |
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| Laboratory practise is focused on mastering fundamental methodology and procedures used in laboratory practice in the fields of synthesis and analysis of chemical substances. Students will get acquainted with fundamental chemical operations and procedures, which are routinely used in chemical syntheses and analyzes in chemical laboratories. |
| Learning Outcomes of the Course Unit |
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| The aim of the course is to get students acquainted with fundamental methodology and procedures used in laboratory practice. |
| Course Contents |
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• Adsorption (adsorption of oxalic acid on active charcoal)
• Rectification (rektification of mixture of methanol/ethanol)
• Thin layer chromatography – determination of vitamins of category B
• Protein separation using discontinuous electrophoresis in a polyacrylamide gel (PAGE)
• Determination of content of phosphoric acid in Coca-Cola
• Determination of content of acetic acid in trade vinegar
• Buffer capacity
• Potentiometric determination of pK
• Optical activity
• Inversion of sucrose
• Spectrophotometric determination of pK of indicator
• Determination of molar absorption coeficient
• Spectrophotometric determination in water analysis (PO43-, NH4+, NO2-, NO3-)
• Volumetric determination in water analysis (CODMn, water hardness Ca2+, Mg2+, acid-base properties)
• Capture and determination of nitrogen oxides in the atmosphere |
| Recommended or Required Reading |
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| Required Reading: |
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| McNair, H. M., Miller, J. M., Basic Gas Chromatography, Second Edition, Wiley-VCH, 2008, ISBN: 9780470439548 |
Otyepková, E. a kol.: Základy vybraných experimentálních chemických metod. VUP Olomouc, 2013.
M. Večeřa, J. Panchartek:. Praktická cvičení z anorganické chemie. SNTL, Praha, 1987.
Hlaváč J., Hradil P., Wiedermannová I., Hejsek M., Nálepa K:. Vybrané úlohy z preparativní organické chemie I. UP Olomouc, 2002.
Dostál V., Šimek J.: Důkaz některých anorganických iontů analytickými reakcemi.. UP, Olomouc, 2000.
Horáková M., Lischke P.: Chemické a fyzikální metody analýzy vod.. SNTL , Praha, 1989.
McNair, H. M., Miller, J. M.: Basic Gas Chromatography, Second Edition, Wiley-VCH, 2008, ISBN: 9780470439548
Nevěčná, T.: Cvičení z fyzikální chemie I, VUP Olomouc, 1990.
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| Recommended Reading: |
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| Hrbáč, J. , Kvítek, L., Nevěčná, T.: Cvičení z fyzikální chemie, VUP Olomouc, 2013. |
| Planned learning activities and teaching methods |
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| Experimental work in labs |
| Assesment methods and criteria |
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| Task Title | Task Type | Maximum Number of Points
(Act. for Subtasks) | Minimum Number of Points for Task Passing |
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| Graded credit | Graded credit | 100 | 51 |